CobaltMaghrebV1, Main, Exploration, bibRecord, 000717

Electrocatalytic oxidation of thiocholine at chemically modified cobalt hexacyanoferrate screen-printed electrodes

Identifieur interne : 000717 ( Main/Exploration ); précédent : 000716; suivant : 000718

Electrocatalytic oxidation of thiocholine at chemically modified cobalt hexacyanoferrate screen-printed electrodes

Auteurs : Fabiana Arduini [Italie] ; Alessio Cassisi [Italie] ; Aziz Amine [Maroc] ; Francesco Ricci [Italie] ; Danila Moscone [Italie] ; Giuseppe Palleschi [Italie]

Source :

Journal of electroanalytical chemistry : (1992) [ 1572-6657 ] ; 2009.

RBID : Pascal:09-0184855

Descripteurs français

Pascal (Inist)
- Electrocatalyse, Oxydation, Cobalt Hexacyanoferrate, Electrocatalyseur, Sérigraphie, Electrode, Détecteur électrochimique, Matériau modifié, Sodium Chlorure, Lithium Chlorure, Potassium Chlorure, Solution tampon, Phosphate, Réaction électrochimique, Thiocholine.
Wicri :
- topic : Phosphate.

English descriptors

KwdEn :
- Buffer solution, Cobalt Hexacyanoferrates, Electrocatalysis, Electrocatalysts, Electrochemical detector, Electrochemical reaction, Electrodes, Lithium Chlorides, Modified material, Oxidation, Phosphates, Potassium Chlorides, Serigraphy, Sodium Chlorides.

Abstract

In this work, cobalt hexacyanoferrate (CoHCF) modified screen-printed electrodes were developed and characterised electrochemically. The effect of different cations was investigated showing a more reversible system with a well-defined peak around +0.35 V vs. Ag/AgCl when Na⁺ was used as cation in the supporting electrolyte. The transfer coefficient (α) and the apparent charge transfer rate constant (k_s) for electron transfer between the electrode and the CoHCF layer was calculated. The electrocatalytic behaviour of CoHCF towards oxidation of enzymatically generated thiocholine was thoroughly investigated. Cyclic voltammetry experiments performed in thiocholine solution showed the classical shape of mediated redox system. The diffusion constant of thiocholine was estimated using chronoamperometry. Also, the catalytic rate constant k of thiocholine at CoHCF-SPE was determined. The current due to thiocholine mediated oxidation was then evaluated in batch amperometric mode at +0.5 V vs. Ag/AgCl obtaining a linear range (5 × 10^-7-1 × 10^-5 mol L^-1) with a low detection limit and a high sensitivity equal to 5 x 10^-7 mol L^-1 and 435 mA mol^-1 L cm^-2, respectively.

Affiliations:

Links toward previous steps (curation, corpus...)

to stream PascalFrancis, to step Corpus: 000111
to stream PascalFrancis, to step Curation: 000184
to stream PascalFrancis, to step Checkpoint: 000112
to stream Main, to step Merge: 000723
to stream Main, to step Curation: 000717

Le document en format XML

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<profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Buffer solution</term>
<term>Cobalt Hexacyanoferrates</term>
<term>Electrocatalysis</term>
<term>Electrocatalysts</term>
<term>Electrochemical detector</term>
<term>Electrochemical reaction</term>
<term>Electrodes</term>
<term>Lithium Chlorides</term>
<term>Modified material</term>
<term>Oxidation</term>
<term>Phosphates</term>
<term>Potassium Chlorides</term>
<term>Serigraphy</term>
<term>Sodium Chlorides</term>
</keywords>
<keywords scheme="Pascal" xml:lang="fr"><term>Electrocatalyse</term>
<term>Oxydation</term>
<term>Cobalt Hexacyanoferrate</term>
<term>Electrocatalyseur</term>
<term>Sérigraphie</term>
<term>Electrode</term>
<term>Détecteur électrochimique</term>
<term>Matériau modifié</term>
<term>Sodium Chlorure</term>
<term>Lithium Chlorure</term>
<term>Potassium Chlorure</term>
<term>Solution tampon</term>
<term>Phosphate</term>
<term>Réaction électrochimique</term>
<term>Thiocholine</term>
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<front><div type="abstract" xml:lang="en">In this work, cobalt hexacyanoferrate (CoHCF) modified screen-printed electrodes were developed and characterised electrochemically. The effect of different cations was investigated showing a more reversible system with a well-defined peak around +0.35 V vs. Ag/AgCl when Na<sup>+</sup>
 was used as cation in the supporting electrolyte. The transfer coefficient (α) and the apparent charge transfer rate constant (k<sub>s</sub>
) for electron transfer between the electrode and the CoHCF layer was calculated. The electrocatalytic behaviour of CoHCF towards oxidation of enzymatically generated thiocholine was thoroughly investigated. Cyclic voltammetry experiments performed in thiocholine solution showed the classical shape of mediated redox system. The diffusion constant of thiocholine was estimated using chronoamperometry. Also, the catalytic rate constant k of thiocholine at CoHCF-SPE was determined. The current due to thiocholine mediated oxidation was then evaluated in batch amperometric mode at +0.5 V vs. Ag/AgCl obtaining a linear range (5 × 10<sup>-7</sup>
-1 × 10<sup>-5</sup>
 mol L<sup>-1</sup>
) with a low detection limit and a high sensitivity equal to 5 x 10<sup>-7</sup>
 mol L<sup>-1</sup>
 and 435 mA mol<sup>-1</sup>
 L cm<sup>-2</sup>
, respectively.</div>
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   |texte=   Electrocatalytic oxidation of thiocholine at chemically modified cobalt hexacyanoferrate screen-printed electrodes
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	Serveur d'exploration sur le cobalt au Maghreb
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Serveur d'exploration sur le cobalt au Maghreb

Electrocatalytic oxidation of thiocholine at chemically modified cobalt hexacyanoferrate screen-printed electrodes

Electrocatalytic oxidation of thiocholine at chemically modified cobalt hexacyanoferrate screen-printed electrodes

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